HRID1654809

反应详情

EQUATION

反应方程式

HRID 1654809 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In 20 ml of ethanol was dissolved 2.70 g (10.0 millimoles) of 2-(2,4-dichlorophenoxy)ethyl bromide, and 1.06 g (10.0 millimoles) of anhydrous sodium carbonate and 3.87 g (30.0 millimoles) of n-octylamine were added to the solution. The mixture was refluxed for 6 hours on an oil bath. After cooling, the reaction mixture was poured into 100 ml of water and extracted with 20 ml of chloroform three times.

WORKUP

后处理

  1. additionwere added to the solution
  2. temperatureThe mixture was refluxed for 6 hours on an oil bath
  3. temperatureAfter cooling
  4. extractionextracted with 20 ml of chloroform three times