HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 20077039, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Phenyl Isothiocyanate | HCID 7673 | — |
| Reactant | 3-[(2-Methylphenyl)methoxy]pyridin-2-amine | HCID 13825882 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20077039 | HCID 20077039 | — |
Reaction Steps
A mixture of 2-amino-3-(2-methylbenzyloxy)pyridine (1.67 g, 0.0078 mol), phenyl isothiocyanate (1.26 g, 0.0093 mol) and toluene (10 ml) was refluxed for 3.5 hours, then cooled and treated with ether to induce crystallisation of the product. Yield 1.8 g (66%), m.p. 150°-151 ° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05409943 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-7f193a063dac4bb1b596cc97d0dffd75 |
| Source note | uspto-grants-1995_04 |