HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 20076930, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Phenyl Isothiocyanate | HCID 7673 | — |
| Reactant | HCID 12758273 | HCID 12758273 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 20076930 | HCID 20076930 | — |
Reaction Steps
A mixture of 2-amino-3-(4-chlorobenzyloxy)pyridine (3.37 g, 0,014 mol), phenyl isothiocyanate (2.33 g, 0,017 mol) and toluene (10 ml) was refluxed for 3.5 hours, then cooled and treated with diethyl ether to induce crystallisation of the product. Yield 4.36 g (82%), m.p. 162°-164 ° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05409943 |
| Source dataset | uspto-grants-1995_04 |
| ORD ID | ord-2d6f9c75c39440e4ac3bd8b4e271dc0c |
| Source note | uspto-grants-1995_04 |