HCID 20077534, compound → HCID 20077527, compound

HRID 1655064Notes

Reaction equation

HRID 1655064 reaction equation
C[O:2][C:3](=[O:33])[CH2:4][C:5]1[C:13]2[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=2)[N:7]([CH2:14][C:15]2[CH:20]=[CH:19][C:18]([O:21][CH2:22][C:23]3[CH:32]=[CH:31][C:30]4[C:25](=[CH:26][CH:27]=[CH:28][CH:29]=4)[N:24]=3)=[CH:17][CH:16]=2)[CH:6]=1.CN1C2C(=CC=C(C(O)=O)C=2)C(CC2C=CC(OCC3C=CC4C(=CC=CC=4)N=3)=CC=2)=C1>>[N:24]1[C:25]2[C:30](=[CH:29][CH:28]=[CH:27][CH:26]=2)[CH:31]=[CH:32][C:23]=1[CH2:22][O:21][C:18]1[CH:17]=[CH:16][C:15]([CH2:14][N:7]2[C:8]3[C:13](=[CH:12][CH:11]=[CH:10][CH:9]=3)[C:5]([CH2:4][C:3]([OH:33])=[O:2])=[CH:6]2)=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 20077534HCID 20077534, compoundHCID 54417574HCID 54417574, compound

Product 1

HCID 20077527HCID 20077527, compound

Procedure

This compound was prepared from the methyl ester (Example 17, part i) by the method described in Example 16, part iii. The product was recrystallised from ethyl acetate, m.p. 163°-166° C.

Workup

  1. customThe product was recrystallised from ethyl acetate, m.p. 163°-166° C.

Sources & evidence

ORD record
ord-486061de799a44ceb3ba694af76ceb07
Source dataset
uspto-grants-1995_04
Patent number
US05410061

Reaction notes

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