HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzhydrylamine → N-(Benzimidazol-2-yl)benzhydrylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzhydrylamine | HCID 7036 | — |
| Reactant | 2-Chlorobenzimidazole | HCID 78572 | — |
| Product | N-(Benzimidazol-2-yl)benzhydrylamine | HCID 11709202 | — |
Reaction Steps
The title compound was prepared from 2-chlorobenzimidazole and benzhydrylamine by Procedure A. The product was isolated by preparative LCMS to give the title compound as the free base (white solid, mp 255-258° C.). MS(ES+) m/z 300 ([M+1]+, 100). 1NMR (DMSO-d6) δ 6.20 (d, 1H), 6.75-7.65 (m, 15H), 10.5 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07737167B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-9cf6243bc6fd45f0a01c176917e554cd |
| Source note | uspto-grants-2010_06 |