HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1655150Generated: October 31, 2026
Thionyl Chloride → 5-Hexylthiophene-2-carboxylic acid chloride
https://huagongshe.com/reaction/1655150
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 5-Hexyl-2-thiophenecarboxylic acid | HCID 13128269 | — |
| Product | 5-Hexylthiophene-2-carboxylic acid chloride | HCID 13128272 | — |
Reaction Steps
10 ml of thionyl chloride was added to 1.0 g (4.72×10-3 ml) of 5-hexylthiophene-2-carboxylic acid, followed by stirring for 4 hours under heating at 80° C. and removal of excessive thionyl chloride by reduced-pressure distillation to obtain 5-hexylthiophene-2-carboxylic chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05250218 |
|---|
| Source dataset | uspto-grants-1993_10 |
|---|
| ORD ID | ord-827cfea01df8488da412d30c3827b6dc |
|---|
| Source note | uspto-grants-1993_10 |
|---|
