HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19386980, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 19386981 | HCID 19386981 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 19386980 | HCID 19386980 | — |
Reaction Steps
A solution of 6-nitro-2,2-dimethyl-3-(2-hydroxyethylamino)methyl-4-(2-oxo-1,2-dihydropyridin-1-yl)-2H-1-benzopyran (0.44 g, 1.18 mmol) in diethylether was treated with excess ethanolic hydrochloric acid (2M) and the resulting precipitate isolated by filtration, to give 0.36 g of 6-nitro-2,2-dimethyl-3-(2-hydroxyethylamino)methyl-4-(2-oxo-1,2-dihydropyridin-1-yl)-2H-1-benzopyran hydrochloride, m.p. 225° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05250547 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-02bd8f69cc1c444dad0206810ac91728 |
| Source note | uspto-grants-1993_10 |