Dimethylformamide → HCID 19792732, compound

Participants

Reaction Steps

The title compound is prepared according to the method of Example 24 using the acid from Example 21 and omitting the dimethylformamide. The crude product is added to ethyl acetate, washed sequentially with saturated sodium bicarbonate and water, dried over magnesium sulfate to give a crude solid. Recrystallization of this solid from acetone affords the desired product as a crystalline solid having a melting point of 145°-146° C.

Provenance & Evidence