HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroquinone → 4-((6-(Acryloyloxy)hexyl)oxy)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroquinone | HCID 785 | — |
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | Acrylic Acid | HCID 6581 | — |
| Reactant | 4-(6-Hydroxyhexyloxy)benzoic acid | HCID 3628413 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 4-((6-(Acryloyloxy)hexyl)oxy)benzoic acid | HCID 3713565 | 55% |
Reaction Steps
4.8 g of 4-(6-hydroxyhexyloxy)benzoic acid and 5.8 g of acrylic acid were heat-refluxed for 40 hours together with 1 ml of sulfuric acid in the presence of hydroquinone in benzene, followed by distilling-off of the solvent and recrystallization to obtain 3.2 g of the product. (Yield: 55 %)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05252251 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-61408abb5d7043ac95f741c90f3ced53 |
| Source note | uspto-grants-1993_10 |