4-Phenyl-3-butenoic acid chloride triethylamine → HCID 178418467, compound

HRID 1656Notes

Reaction equation

HRID 1656 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[CH:10]=[CH:9][C:8]([C@H:11]2[CH2:16][CH2:15][C@H:14]([OH:17])[CH2:13][CH2:12]2)=[CH:7][CH:6]=1)[CH3:3].[C:18]1([CH:24]=[CH:25][CH2:26][C:27](Cl)=[O:28])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1.C(N(CC)CC)C>>[C:18]1([CH:24]=[CH:25][CH2:26][C:27]([O:17][C@H:14]2[CH2:15][CH2:16][C@H:11]([C:8]3[CH:9]=[CH:10][C:5]([CH2:4][N:2]([CH3:1])[CH3:3])=[CH:6][CH:7]=3)[CH2:12][CH2:13]2)=[O:28])[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

3

Reactant 2

HCID 1317205564-Phenyl-3-butenoic acid chloride triethylamineHCID 178418401HCID 178418401, compound

Product 1

HCID 178418467HCID 178418467, compound

Procedure

from trans-4-(4-dimethylaminomethylphenyl)-cyclohexanol and 4-phenyl-3-butenoic acid chloride/triethylamine. White crystals.

Sources & evidence

ORD record
ord-fb382a38ecde4b3498d73cf8d48e3315
Source dataset
uspto-grants-1998_03
Patent number
US05726205

Reaction notes

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