HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Diaminotoluene → (R)-N-(5-Methylbenzimidazol-2-y1)-1,2,3,4-tetrahydro-1-naphthylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Diaminotoluene | HCID 10332 | — |
| Reactant | (R)-1-isothiocyanato-1,2,3,4-tetrahydronaphthalene | HCID 24946216 | — |
| Product | (R)-N-(5-Methylbenzimidazol-2-y1)-1,2,3,4-tetrahydro-1-naphthylamine | HCID 11507385 | — |
Reaction Steps
The title compound was prepared from 3,4-diaminotoluene and (R)-1-isothiocyanato-1,2,3,4-tetrahydronaphthalene by Procedure D. The title compound was isolated by column chromatography as the free base (off-white solid, mp 91-93° C.). MS(ES+) m/z 278 ([M+1]+, 100).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07737167B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-f4a78d4171934ed387cd23e251575514 |
| Source note | uspto-grants-2010_06 |