HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Cyclohexanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Cyclohexene | HCID 8079 | — |
| Solvent | Water | HCID 962 | — |
| Product | Cyclohexanol | HCID 7966 | — |
| Product | Cyclohexyl acetate | HCID 12146 | — |
Reaction Steps
Japanese Patent Application Laid-open No. 313447/1989 discloses an addition reaction of acetic acid with cyclohexene in the presence of both ZSM-5, a high silica content-zeolite, as a catalyst and water. According to this method, the reaction temperature is 120° C. and the reaction time is 4 hours resulting in the formation of cyclohexanol in a 12.5% yield and cyclohexyl acetate at most in a 65% yield. The reaction temperature is high and the catalytic activity is low.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05254721 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-96fbb1c681c049e4938f24f20345ff54 |
| Source note | uspto-grants-1993_10 |