Acetic Acid → Cyclohexyl acetate
Reaction equation
[CH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.[C:7]([OH:10])(=[O:9])[CH3:8]>>[C:7]([O:10][CH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)(=[O:9])[CH3:8]Participants
3
Reactant 2
Product 1
Conditions
- Temperature
- 100 °C
Procedure
In a 200 ml autoclave were placed the above-mentioned commercially available dodecatungstosilicic acid 5.0 g, the above-mentioned commercially available acetic acid 61.5 g and the above-mentioned commercially available cyclohexene 13.5 g and nitrogen gas was fed thereinto until the pressure reached 5 kg/cm2 (gauge), and then a reaction was carried out with stirring by heating at 100° C. for 1 hour. The result is shown in Table 1, that is, cyclohexyl acetate was produced in high yield.
Sources & evidence
- ORD record
- ord-2f286c5fefe54f32acc08d8c9b5ac991
- Source dataset
- uspto-grants-1993_10
- Patent number
- US05254721
Reaction notes
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