Acetic Acid → Cyclohexyl acetate

HRID 1656787Notes

Reaction equation

HRID 1656787 reaction equation
[CH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH:2]=1.[C:7]([OH:10])(=[O:9])[CH3:8]>>[C:7]([O:10][CH:1]1[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1)(=[O:9])[CH3:8]

Participants

3

Reactant 2

HCID 176Acetic AcidHCID 8079Cyclohexene

Product 1

HCID 12146Cyclohexyl acetate

Procedure

The procedure of Example 16 was repeated to conduct the reaction of acetic acid with cyclohexene except that the reaction temperature was 130° C. and the reaction time was 0.5 hour. The result is shown in Table 3, that is, cyclohexyl acetate was produced in high yield within a short time.

Workup

  1. customwas 130° C.

Sources & evidence

ORD record
ord-5cd294b441c949538efed39bee9179cf
Source dataset
uspto-grants-1993_10
Patent number
US05254721

Reaction notes

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