Sodium hydride → HCID 23719342, compound

Participants

Reaction Steps

A solution of the 2,6-bis(1-methylethyl)phenyl[(dibutylamino)sulfonyl]carbamate (5.5 g, 13.3 mmol) in 75 mL tetrahydrofuran was added dropwise to a suspension of sodium hydride (0.4 g, 80% dispersion in mineral oil, 13.3 mmol) in 50 mL tetrahydrofuran at 0° C. under an atmosphere of nitrogen. Stirred for 3 hours, gradually warming to room temperature. Concentrated in vacuo and triturated with hexanes to give the title compound, mp 162°-166° C.

Provenance & Evidence