Sulfuric Acid → HCID 19788883, compound

HRID 1656840Notes

Reaction equation

HRID 1656840 reaction equation
[F:1][CH2:2][C:3]([CH:7]([F:9])[F:8])=[C:4]([F:6])[F:5].S(=O)(=O)(O)[OH:11]>O>[F:1][CH2:2][C:3]([OH:11])([CH:7]([F:9])[F:8])[CH:4]([F:6])[F:5]

Participants

4

Reactant 2

HCID 1118Sulfuric AcidHCID 19788885HCID 19788885, compound

Product 1

HCID 19788883HCID 19788883, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

As another example, 2-fluoromethyl-1,1,3,3-tetrafluoro-2-propanol may be prepared by fluorinating commercially available 1,1,3-trichloro-2-propanone to form 1,1,3-trifluoro-2-propanone which may then be reacted with CF2 carbene to form 2-fluoromethyl-1,1,3,3-tetrafluoro-1-propene. The 2-fluoromethyl-1,1,3,3-tetrafluoro-1-propene may then be reacted with sulfuric acid and then water to form 2-fluoromethyl-1,1,3,3-tetrafluoro-2-propanol.

Sources & evidence

ORD record
ord-d59c28286ad041a2ae03717d5c804e3c
Source dataset
uspto-grants-1993_10
Patent number
US05254755

Reaction notes

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