HRID1657179

反应详情

EQUATION

反应方程式

HRID 1657179 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

An admixture of 4.7 grams of 4-[4'-(2"-hydroxyethyl)piperazino]benzaldehyde (0.02 mol), 3.0 grams of 3-aminorhodanine (0.02 mol), toluene (30 mL), and glacial acetic acid (5 mL) was refluxed for 4 hours. The admixture was then cooled to room temperature and the solvent was decanted. The remaining paste was triturated with ethanol and then filtered off and dried.

WORKUP

后处理

  1. customthe solvent was decanted
  2. customThe remaining paste was triturated with ethanol
  3. filtrationfiltered off
  4. customdried