HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → N-t-butyl-4,4-diphenyl-2-cyclopentenylamine hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | N-t-butyl-4,4-diphenyl-2-cyclopentenylamine | HCID 9796063 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N-t-butyl-4,4-diphenyl-2-cyclopentenylamine hydrochloride | HCID 19787440 | — |
Reaction Steps
To a solution of (-)-N-t-butyl-4,4-diphenyl-2-cyclopentenylamine (8.82 g) in diethyl ether (50 ml) was added water (15 ml) and conc. hydrochloric acid (5 ml) at 0°-10° C. and stirred for 30 minutes. The resulting precipitate was collected by filtration and washed with diethyl ether to give (-)-N-t-butyl-4,4-diphenyl-2-cyclopentenylamine hydrochloride (9.70 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05256824 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-9e9b48e21d5b4ccc81a663b84f29b07d |
| Source note | uspto-grants-1993_10 |