HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitromethane → HCID 54458408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | HCID 15187043 | HCID 15187043 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54458408 | HCID 54458408 | — |
Reaction Steps
A mixture of 3-benzyl-2-indolecarbaldehyde (7.06 g), ammonium acetate (462 mg) and nitromethane (10.5 ml) in methanol (30 ml) was refluxed for 2 hours. After cooling, precipitates formed were collected and washed two times with chilled methanol (5 ml) to give 3-benzyl-2-(2-nitrovinyl)indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05256780 |
| Source dataset | uspto-grants-1993_10 |
| ORD ID | ord-064abf21f394428c893a0f90ca590d2f |
| Source note | uspto-grants-1993_10 |