HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1,2,4-trichloro-3-(chloromethyl)- → 2-(2,3,6-trichlorophenylmethylthio)pyridine N-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1,2,4-trichloro-3-(chloromethyl)- | HCID 74022 | — |
| Reactant | HCID 178507102 | HCID 178507102 | — |
| Product | 2-(2,3,6-trichlorophenylmethylthio)pyridine N-oxide | HCID 54210758 | — |
Reaction Steps
The compound 2-(2,3,6-trichlorophenylmethylthio)-pyridine N-oxide is prepared from 2,3,6-trichlorobenzylchloride and 2-mercaptopyridine N-oxide sodium salt by the procedure employed in Example 1. Melting point 232° - 234°C. Yield quantative. Structure confirmed by IR and NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960542 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-7bea918b37a748359b51923d4e385da1 |
| Source note | uspto-grants-1976_06 |