HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Tetradecanol → HCID 54222431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Tetradecanol | HCID 8209 | — |
| Reactant | HCID 54202627 | HCID 54202627 | — |
| Catalyst | Titanium tetrabutoxide | HCID 21801 | — |
| Product | HCID 54222431 | HCID 54222431 | — |
Reaction Steps
1-(2,6 -Dichloro-4-methoxycarbonylphenyl)-3-benzamido-5-pyrazolone prepared by the method as described in step (1) was reacted with 1-tetradecanol in the presence of butyl titanate as catalyst in a manner similar to Synthesis Example 1 to obtain the desired coupler, 1-(2,6 -dichloro-4-n-tetradecyloxycarbonylphenyl)-3-benzamido-5-pyrazolone as colorless crystals. The melting point of the product as 146°-147°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960571 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-a76303c54acb452f9f4af28c8f73c118 |
| Source note | uspto-grants-1976_06 |