Ammonia → HCID 53983678, compound

HRID 1657419Notes

Reaction equation

HRID 1657419 reaction equation
[C:1]1([CH2:17][C:18]([OH:20])=O)[C:14]2[C:13](=[O:15])[C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[C:6](=[O:16])[C:5]=2[CH:4]=[CH:3][CH:2]=1.[NH3:21]>>[C:1]1([CH2:17][C:18]([NH2:21])=[O:20])[C:14]2[C:13](=[O:15])[C:12]3[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=3)[C:6](=[O:16])[C:5]=2[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 222AmmoniaHCID 12260948HCID 12260948, compound

Product 1

HCID 53983678HCID 53983678, compound

Procedure

Under the stated conditions, the ester of anthraquinone-acetic acid reacts with the NH3 to form, directly, the 1-aza-2-hydroxybenzanthrone, without the necessity of isolating the intermediate product 1-anthraquinone acetamide.

Workup

  1. customto form

Sources & evidence

ORD record
ord-6726010707bc4165819c3e4185245275
Source dataset
uspto-grants-1976_06
Patent number
US03960866

Reaction notes

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