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HRID1657508

反应详情

EQUATION

反应方程式

HRID 1657508 的结构方程式

REACTANTS

反应物

2
结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

结构：O=C(CCCCCC(=O)[c-]1cccc1)c1ccccc1.[Fe+2].c1cc[cH-]c1
HCID178520604

未命名化合物

PRODUCTS

生成物

1
结构：O=C([c-]1cccc1)C1CCCCC1(O)c1ccccc1.[Fe+2].c1cc[cH-]c1
HCID178519396

未命名化合物

收率 47%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

6-Benzoylhexanoylferrocene [2.91g; 7.5 mmole] was dissolved in a solution of sodium hydroxide [0.3g; 7.5 mmole] in ethanol [100 ml ] and stirred at room temperature for 16 hours. Filtration and recrystallization from cyclohexanone gave the desired product [1.3g; 47%] mp 172°-3°C.

WORKUP

后处理

  1. filtrationFiltration and recrystallization from cyclohexanone