HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl acetate → Methallyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl acetate | HCID 11584 | — |
| Reactant | 2-Methylallyl acetate | HCID 69962 | — |
| Product | Methyl Acetate | HCID 6584 | 93% |
| Product | Methallyl alcohol | HCID 10557 | 99% |
Reaction Steps
The tube, catalyst and general procedure described in Example 2 were employed, with 57.0 g of methallyl acetate substituted for the allyl acetate. The effluent in this case was composed of 12.5 g of unconverted methallyl acetate (22% recovery), 27.8 g of methallyl alcohol (99% yield based on 78% conversion), 26.8 g of methyl acetate (93% yield) and the excess methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960971 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-25425321457e44eb8cba76fdee0b2751 |
| Source note | uspto-grants-1976_06 |