HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl acetate → 2-Buten-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl acetate | HCID 11584 | — |
| Reactant | 2-Buten-1-yl acetate | HCID 81620 | — |
| Product | Methyl Acetate | HCID 6584 | 85% |
| Product | 2-Buten-1-ol | HCID 20024 | 88% |
Reaction Steps
The tube, catalyst and general procedure described in Example I were employed, with 57.0 g of crotyl acetate substituted for the allyl acetate. The effluent in this case was composed of 12.5 g of unconverted crotyl acetate (22% recovery), 24.7 g of crotyl alcohol (88% yield based on 78% conversion), 24.5 g of methyl acetate (85% yield) and the excess methanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03960971 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-896d844fcae34f0f9f0f53a02c04ab5a |
| Source note | uspto-grants-1976_06 |