反应详情

A mixture of 22.8 gm. (0.1 mole) of thiocarbanilide and 17 gm. (0.12 mole) of methyl iodide in 400 ml. of ethanol is heated at reflux for 6 hours. The solvent is evaporated and residue is crystallized from ethyl acetate; 29 gm. (78%), m.p. 155°-156°.

1. additionA mixture of 22.8 gm
2. temperatureat reflux for 6 hours
3. customThe solvent is evaporated
4. customresidue is crystallized from ethyl acetate