Isopropyl iodide → HCID 21534846, compound

HRID 1657602Notes

Reaction equation

HRID 1657602 reaction equation
I[CH:2]([CH3:4])[CH3:3].[OH:5][C:6]1[CH:19]=[CH:18][C:17]2[S:16][C:15]3[C:10](=[CH:11][CH:12]=[CH:13][C:14]=3[S:20]([CH3:23])(=[O:22])=[O:21])[NH:9][C:8]=2[CH:7]=1>>[CH:2]([O:5][C:6]1[CH:19]=[CH:18][C:17]2[S:16][C:15]3[C:10](=[CH:11][CH:12]=[CH:13][C:14]=3[S:20]([CH3:23])(=[O:22])=[O:21])[NH:9][C:8]=2[CH:7]=1)([CH3:4])[CH3:3]

Participants

3

Reactant 2

HCID 6362Isopropyl iodideHCID 21534837HCID 21534837, compound

Product 1

HCID 21534846HCID 21534846, compoundYield 99.9%

Procedure

2-Isopropoxy-6-methylsulphonylphenothiazine (21.7 g.) is prepared by reacting 2-iodopropane (17.0 g.) with 2-hydroxy-6-methylsulphonylphenothiazine (m.p. 218°-219°C.; 19.0 g.).

Sources & evidence

ORD record
ord-5255eb38105d45cfb56de1e898d806f5
Source dataset
uspto-grants-1976_06
Patent number
US03961055

Reaction notes

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