Benzyl Chloride → HCID 21534823, compound

HRID 1657606Notes

Reaction equation

HRID 1657606 reaction equation
[CH2:1](Cl)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[OH:9][C:10]1[CH:23]=[CH:22][C:21]2[S:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][C:18]=3[S:24](=[O:29])(=[O:28])[N:25]([CH3:27])[CH3:26])[NH:13][C:12]=2[CH:11]=1>>[CH2:1]([O:9][C:10]1[CH:23]=[CH:22][C:21]2[S:20][C:19]3[C:14](=[CH:15][CH:16]=[CH:17][C:18]=3[S:24](=[O:29])(=[O:28])[N:25]([CH3:26])[CH3:27])[NH:13][C:12]=2[CH:11]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 7503Benzyl ChlorideHCID 215348332-Hydroxy-6-dimethylsulphamoylphenothiazine

Product 1

HCID 21534823HCID 21534823, compoundYield 27%

Procedure

2-Benzyloxy-6-dimethylsulphamoylphenothiazine (m.p. 192°-194°C.; 69.0 g.) is prepared by reacting benzyl chloride (106.0 g.) with 2-hydroxy-6-dimethylsulphamoylphenothiazine (200 g.).

Sources & evidence

ORD record
ord-d275c815b18a43659681acd5929f8492
Source dataset
uspto-grants-1976_06
Patent number
US03961055

Reaction notes

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