HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21421182, compound → HCID 21421206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21421182 | HCID 21421182 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21421206 | HCID 21421206 | — |
Reaction Steps
1-(2-Nitro-4-chlorophenoxy)-2-hydroxy-3-tert.-butylamino propane was hydrogenated in the presence of Raney-nickel in methanol to obtain 1-(2-amino-4-chlorophenoxy)-2-hydroxy-3-tert.-butylamino propane dihydrochloride having a melting point of 260°-262°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03961071 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-073d1f5731fe4b3ab4c4234e25cfed6e |
| Source note | uspto-grants-1976_06 |