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HRID1657692

反应详情

EQUATION

反应方程式

HRID 1657692 的结构方程式

REACTANTS

反应物

2
结构：CN(C)CCCNN
HCID120423

3-Hydrazinyl-N,N-dimethyl-1-propanamine

C5H15N3

结构：O=C1C(=Cc2ccccc2)CSCC1=Cc1ccccc1
HCID336779

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)CCCN1N=C2C(=Cc3ccccc3)CSCC2C1c1ccccc1
HCID53921981

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

Tetrahydro-3,5-bis-(phenylmethylene)-4H-thiopyran-4-one (5g) is refluxed with 2.1g of 3-dimethylaminopropylhydrazine in 50ml of methanol for 4 hours. The solvent is evaporated off and the residue is crystallized from 30ml of acetonitrile to yield 3.9g of the title compound, melting point 83°-85°C.

WORKUP

后处理

  1. customThe solvent is evaporated off
  2. customthe residue is crystallized from 30ml of acetonitrile