2-Furancarbonyl chloride → HCID 21530229, compound

HRID 1657758Notes

Reaction equation

HRID 1657758 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[C:6](Cl)=[O:7].[C:9]1([CH2:15][CH2:16][CH2:17][N:18]2[CH2:23][CH2:22][NH:21][CH2:20][CH:19]2[CH3:24])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>C(Cl)(Cl)Cl>[C:9]1([CH2:15][CH2:16][CH2:17][N:18]2[CH2:23][CH2:22][N:21]([C:6]([C:2]3[O:1][CH:5]=[CH:4][CH:3]=3)=[O:7])[CH2:20][CH:19]2[CH3:24])[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 21530230HCID 21530230, compound

Product 1

HCID 21530229HCID 21530229, compound

Reagents, catalysts & solvents 1

HCID 6212ChloroformSolvent

Procedure

2-Furoyl chloride (1.5 g) was added dropwise with stirring to a solution of 1-(3-phenylpropyl)-2-methylpiperazine [b.p. 138° - 140°C (8 mmHg)] (2.2 g) and CHCl3 (100 ml).

Sources & evidence

ORD record
ord-360f3112dc2f40319cce3d42b0a6bf0c
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

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