2-Furancarbonyl chloride → HCID 21530261, compound

HRID 1657761Notes

Reaction equation

HRID 1657761 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][CH2:10][N:11]1[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]1.[O:17]1[CH:21]=[CH:20][CH:19]=[C:18]1[C:22]([Cl:24])=[O:23]>C1C=CC=CC=1>[ClH:24].[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][CH2:10][N:11]1[CH2:12][CH2:13][N:14]([C:22]([C:18]2[O:17][CH:21]=[CH:20][CH:19]=2)=[O:23])[CH2:15][CH2:16]1

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 21530234HCID 21530234, compound

Product 1

HCID 21530261HCID 21530261, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 2 from a mixture of 1-[3-(o-methylphenyl)propyl]piperazine [b.p. 135° - 136°C (2 mmHg), dihydrochloride, m.p. 240° - 245°C], 2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-5e4eb33b3acc4b069890394adcc77b75
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

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