2-Furancarbonyl chloride → HCID 21530265, compound

HRID 1657762Notes

Reaction equation

HRID 1657762 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][CH2:9][CH2:10][N:11]2[CH2:16][CH2:15][NH:14][CH2:13][CH2:12]2)[CH:5]=[CH:6][CH:7]=1.[O:17]1[CH:21]=[CH:20][CH:19]=[C:18]1[C:22]([Cl:24])=[O:23]>C1C=CC=CC=1>[ClH:24].[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][CH2:9][CH2:10][N:11]2[CH2:12][CH2:13][N:14]([C:22]([C:18]3[O:17][CH:21]=[CH:20][CH:19]=3)=[O:23])[CH2:15][CH2:16]2)[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 215302251-[3-(3-Methylphenyl)propyl]piperazine

Product 1

HCID 21530265HCID 21530265, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 1 from a mixture of 1-[3-(m-methylphenyl)propyl]piperazine [b.p. 137° - 145°C (2 mmHg), dihydrochloride, m.p. 237°C], 2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-63632fc86bca49e083712b72d058bd49
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

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