2-Furancarbonyl chloride → HCID 21530285, compound
Reaction equation
[CH2:1]([O:3][C:4]1[CH:9]=[CH:8][C:7]([CH2:10][CH2:11][CH2:12][N:13]2[CH2:18][CH2:17][NH:16][CH2:15][CH2:14]2)=[CH:6][CH:5]=1)[CH3:2].[O:19]1[CH:23]=[CH:22][CH:21]=[C:20]1[C:24]([Cl:26])=[O:25]>C1C=CC=CC=1>[ClH:26].[CH2:1]([O:3][C:4]1[CH:5]=[CH:6][C:7]([CH2:10][CH2:11][CH2:12][N:13]2[CH2:18][CH2:17][N:16]([C:24]([C:20]3[O:19][CH:23]=[CH:22][CH:21]=3)=[O:25])[CH2:15][CH2:14]2)=[CH:8][CH:9]=1)[CH3:2]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
The compound was obtained by following the same process as in Example 2 from a mixture of 1-[3-(p-ethoxyphenyl)propyl]piperazine [b.p. 162° - 165°C (4 mmHg), dihydrochloride, m.p. 232° - 239°C], 2-furoyl chloride and benzene.
Workup
- customThe compound was obtained
Sources & evidence
- ORD record
- ord-477d943e9cd64f8d9e3d8da8c00744ec
- Source dataset
- uspto-grants-1976_06
- Patent number
- US03962249
Reaction notes
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