2-Furancarbonyl chloride → HCID 68131291, compound

HRID 1657767Notes

Reaction equation

HRID 1657767 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][N:10]2[CH2:15][CH2:14][NH:13][C@H:12]([CH3:16])[C@@H:11]2[CH3:17])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[O:18]1[CH:22]=[CH:21][CH:20]=[C:19]1[C:23]([Cl:25])=[O:24]>C1C=CC=CC=1>[ClH:25].[C:1]1([CH2:7][CH2:8][CH2:9][N:10]2[CH2:15][CH2:14][N:13]([C:23]([C:19]3[O:18][CH:22]=[CH:21][CH:20]=3)=[O:24])[C@H:12]([CH3:16])[C@@H:11]2[CH3:17])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 68130936HCID 68130936, compound

Product 1

HCID 68131291HCID 68131291, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 1 from a mixture of cis-1-(3-phenylpropyl)-2,3-dimethylpiperazine [b.p. 126° - 128°C (2 mmHg), dipicrate, m.p. 227° - 228°C], 2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-fc9b0c58b6364f8384352796b20889ac
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

Loading…