2-Furancarbonyl chloride → HCID 68130982, compound

HRID 1657768Notes

Reaction equation

HRID 1657768 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][CH2:10][N:11]1[CH2:16][C@@H:15]([CH3:17])[NH:14][CH2:13][C@@H:12]1[CH3:18].[O:19]1[CH:23]=[CH:22][CH:21]=[C:20]1[C:24]([Cl:26])=[O:25]>C1C=CC=CC=1>[ClH:26].[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][CH2:10][N:11]1[CH2:16][C@@H:15]([CH3:17])[N:14]([C:24]([C:20]2[O:19][CH:23]=[CH:22][CH:21]=2)=[O:25])[CH2:13][C@@H:12]1[CH3:18]

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 68130897HCID 68130897, compound

Product 1

HCID 68130982HCID 68130982, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 2 from a mixture of trans-1-[3-(o-methylphenyl)propyl]-2,5-dimethylpiperazine [b.p. 130° - 140°C (4 mmHg), dipicrate, 250° - 252°C], 2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-234b282704d9437bb72aec82c45e6e27
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

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