2-Furancarbonyl chloride → HCID 68131241, compound

HRID 1657769Notes

Reaction equation

HRID 1657769 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][CH2:9][CH2:10][N:11]2[CH2:16][C@@H:15]([CH3:17])[NH:14][CH2:13][C@@H:12]2[CH3:18])[CH:5]=[CH:6][CH:7]=1.[O:19]1[CH:23]=[CH:22][CH:21]=[C:20]1[C:24]([Cl:26])=[O:25]>C1C=CC=CC=1>[ClH:26].[CH3:1][C:2]1[CH:3]=[C:4]([CH2:8][CH2:9][CH2:10][N:11]2[CH2:16][C@@H:15]([CH3:17])[N:14]([C:24]([C:20]3[O:19][CH:23]=[CH:22][CH:21]=3)=[O:25])[CH2:13][C@@H:12]2[CH3:18])[CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 68132409HCID 68132409, compound

Product 1

HCID 68131241HCID 68131241, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 2 from a mixture of trans-1-[3-(m-methylphenyl)propyl]-2,5-dimethylpiperazine [b.p. 125° - 132°C (4 mmHg), dipicrate, m.p. 245° - 248°C], 2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-a741e11adba24a998e750d06cf37dc46
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

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