2-Furancarbonyl chloride → HCID 68131096, compound

HRID 1657770Notes

Reaction equation

HRID 1657770 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][N:10]2[CH2:15][CH2:14][NH:13][C@@H:12]([CH3:16])[C@@H:11]2[CH3:17])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[O:18]1[CH:22]=[CH:21][CH:20]=[C:19]1[C:23](Cl)=[O:24]>C1C=CC=CC=1>[C:1]1([CH2:7][CH2:8][CH2:9][N:10]2[CH2:15][CH2:14][N:13]([C:23]([C:19]3[O:18][CH:22]=[CH:21][CH:20]=3)=[O:24])[C@@H:12]([CH3:16])[C@@H:11]2[CH3:17])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 70631641(2S,3S)-2,3-Dimethyl-1-(3-phenylpropyl)piperazine

Product 1

HCID 68131096HCID 68131096, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 3 from a mixture of trans-1-(3-phenylpropyl)-2,3-dimethylpiperazine [b.p. 130° - 132°C (2 mmHg), dipicrate, m.p. 195° - 196°C], 2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-beb57f498ab74df08a7747ac6cdcf906
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

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