2-Furancarbonyl chloride → HCID 68132439, compound

HRID 1657771Notes

Reaction equation

HRID 1657771 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH2:9][CH2:10][CH2:11][N:12]1[CH2:17][C@@H:16]([CH3:18])[NH:15][CH2:14][C@@H:13]1[CH3:19].[O:20]1[CH:24]=[CH:23][CH:22]=[C:21]1[C:25]([Cl:27])=[O:26]>C1C=CC=CC=1>[ClH:27].[CH3:1][O:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][C:4]=1[CH2:9][CH2:10][CH2:11][N:12]1[CH2:17][C@@H:16]([CH3:18])[N:15]([C:25]([C:21]2[O:20][CH:24]=[CH:23][CH:22]=2)=[O:26])[CH2:14][C@@H:13]1[CH3:19]

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 68130368HCID 68130368, compound

Product 1

HCID 68132439HCID 68132439, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 2 from a mixture of trans-1-[3-(o-methoxyphenyl)propyl]-2,5-dimethylpiperazine [b.p. 146° - 150°C (2 mmHg), dipicrate, m.p. 260° - 265°C], 2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-7c033bee044e45e7a995a3a6a6b87c41
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

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