2-Furancarbonyl chloride → HCID 21530223, compound

HRID 1657772Notes

Reaction equation

HRID 1657772 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][CH2:10][N:11]1[CH2:16][CH2:15][NH:14][CH:13]([CH3:17])[CH2:12]1.[O:18]1[CH:22]=[CH:21][CH:20]=[C:19]1[C:23]([Cl:25])=[O:24]>C1C=CC=CC=1>[ClH:25].[CH3:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:8][CH2:9][CH2:10][N:11]1[CH2:16][CH2:15][N:14]([C:23]([C:19]2[O:18][CH:22]=[CH:21][CH:20]=2)=[O:24])[CH:13]([CH3:17])[CH2:12]1

Participants

4

Reactant 2

HCID 682422-Furancarbonyl chlorideHCID 21530231HCID 21530231, compound

Product 1

HCID 21530223HCID 21530223, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 2 from a mixture of 1-[3-(o-methylphenyl)propyl]-3-methylpiperazine [b.p. 120° - 125°C (2 mmHg), dipicrate, m.p. 245° - 250°C], 2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-12e9f478e2e04be2a79aebf744b1388d
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

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