3-Methylfuran-2-carbonyl chloride → 1-(3-Phenylpropyl)-3-methyl-4-(3-methyl-2-furoyl)piperazine hydrochloride

HRID 1657778Notes

Reaction equation

HRID 1657778 reaction equation
[C:1]1([CH2:7][CH2:8][CH2:9][N:10]2[CH2:15][CH2:14][NH:13][CH:12]([CH3:16])[CH2:11]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:17][C:18]1[CH:22]=[CH:21][O:20][C:19]=1[C:23]([Cl:25])=[O:24]>C1C=CC=CC=1>[ClH:25].[C:1]1([CH2:7][CH2:8][CH2:9][N:10]2[CH2:15][CH2:14][N:13]([C:23]([C:19]3[O:20][CH:21]=[CH:22][C:18]=3[CH3:17])=[O:24])[CH:12]([CH3:16])[CH2:11]2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 27966743-Methylfuran-2-carbonyl chlorideHCID 215302811-(3-Phenylpropyl)-3-methylpiperazine

Product 1

HCID 215302731-(3-Phenylpropyl)-3-methyl-4-(3-methyl-2-furoyl)piperazine hydrochloride

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

The compound was obtained by following the same process as in Example 2 from a mixture of 1-(3-phenylpropyl)-3-methylpiperazine, 3-methyl-2-furoyl chloride and benzene.

Workup

  1. customThe compound was obtained

Sources & evidence

ORD record
ord-b926999bb7ff4ef0b3ca838b7b81b981
Source dataset
uspto-grants-1976_06
Patent number
US03962249

Reaction notes

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