HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allyl isocyanate → HCID 54445625, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allyl isocyanate | HCID 15123 | — |
| Reactant | 2,2,7,7-Tetramethyl-1,4-diazepan-5-one | HCID 546910 | — |
| Product | HCID 54445625 | HCID 54445625 | — |
Reaction Steps
Using the same conditions as in Example 4, 17 parts of 2,2,7,7-tetramethyl-1,4-diazacycloheptan-5-one and 9 parts of allyl isocyanate afforded 26 parts of 4-allylcarbamoyl-2,2,7,7-tetramethyl-1,4-diazacycloheptan-5-one which was purified by distillation at 131°-135°C and 0.3mm pressure. The colourless oil gave the following elemental analysis by weight:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962255 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-6e61d5e25a67468390d3857872c53902 |
| Source note | uspto-grants-1976_06 |