HRID1657840

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID24386

Thionyl chloride

Cl2OS

HCID12319365

2-Bromo-N-(1-hydroxy-2-methylpropan-2-yl)-4,5-dimethoxybenzamide

C13H18BrNO4

PRODUCTS

生成物

HCID12319367

2-(2-Bromo-4,5-dimethoxyphenyl)-4,4-dimethyl-4,5-dihydro-1,3-oxazole

C13H16BrNO3

PROCEDURE

实验过程

Reaction of 2-bromo-4,5-dimethoxy-N-(1-hydroxy-2-methyl-2-propyl)benzamide and thionyl chloride by the method described in Example 1b provides 2-(2-bromo-4,5-dimethoxyphenyl)-4,4-dimethyl-2-oxazoline as colorless crystals, m.p. 49°-51°.