Thionyl Chloride → HCID 53824524, compound

HRID 1657907Notes

Reaction equation

HRID 1657907 reaction equation
[CH3:1][C:2]1[C:7]([C:8](=[O:16])[C:9]2[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][CH:10]=2)=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:17][C:18]([OH:20])=O.S(Cl)([Cl:23])=O>>[CH3:1][C:2]1[C:7]([C:8](=[O:16])[C:9]2[CH:14]=[CH:13][C:12]([Cl:15])=[CH:11][CH:10]=2)=[CH:6][CH:5]=[CH:4][C:3]=1[CH2:17][C:18]([Cl:23])=[O:20]

Participants

3

Reactant 2

HCID 24386Thionyl Chloride2×HCID 20455613HCID 20455613, compound

Product 1

HCID 53824524HCID 53824524, compound

Procedure

A solution of 5.8 g of 2-methyl-3-(p-chlorobenzoyl)-phenylacetic acid in 25 ml of thionyl chloride was refluxed for 11/2 hours and excess thionyl chloride was removed to obtain 2-methyl-3-(p-chlorobenzoyl)-phenylacetic acid chloride melting at 62°-63°C.

Workup

  1. customwas removed

Sources & evidence

ORD record
ord-e73b13296b2644dc9aae64883db29210
Source dataset
uspto-grants-1976_06
Patent number
US03962303

Reaction notes

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