Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (E)-2-Nonenoic Acid | HCID 5312586 | — |
| Product | HCID 12575251 | HCID 12575251 | 91% |
Reaction Steps
Thionyl chloride (131 g, 1.1 mole) is added to trans-2-nonenoic acid (156 g, 1.0 mole). Reaction occurs immediately with the evolution of HCl and SO2. After the initial reaction subsides, the mixture is heated slowly to 130°C. The dark mixture is vacuum distilled to yield trans-2-nonenoyl chloride, b.p. 90°C/2 mm, 155 g, 91% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US03962321 |
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| Source dataset | uspto-grants-1976_06 |
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| ORD ID | ord-571b4d0b56cf47a3b7999232a4246a05 |
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| Source note | uspto-grants-1976_06 |
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