化工社化工社 化学情報印刷レポート · 研究参考用
O-Cymene → Benzene, 1-(chloromethyl)-2-(1-methylethenyl)-
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | O-Cymene | HCID 10703 | — |
| 反応物 | 1-(Chloromethyl)-2-ethenylbenzene | HCID 89757 | — |
| 反応物 | Chloromethyl chloroisopropyl benzene | HCID 14555442 | — |
| 生成物 | Benzene, 1-(chloromethyl)-2-(1-methylethenyl)- | HCID 11491997 | — |
反応手順
Finally the art teaches in U.S. Pat. No. 2,780,604 that chloromethyl vinyl benzene can be prepared via a two step liquid phase reaction whereby isopropyl toluene is chlorinated via ultraviolent light and the subsequently distilled chloromethyl chloroisopropyl benzene is dehydrohalogenated with heat to give chloromethylisopropenylbenzene.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US03962357 |
| 出典データセット | uspto-grants-1976_06 |
| ORD ID | ord-65ca56ebc22b44329d9dc8e3e67cb5eb |
| 出典メモ | uspto-grants-1976_06 |