HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 54295138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Sulfuric acid magnesium salt (1:1) | HCID 24083 | — |
| Reactant | HCID 21529925 | HCID 21529925 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54295138 | HCID 54295138 | — |
Reaction Steps
A mixture of dibutyl aminomethylphosphonate (69.7 g) and benzaldehyde (33.0 g) in benzene (600 ml) is stirred with magnesium sulfate (150 g) for 3 hours. The mixture is filtered and the salts washed with benzene. Concentration of the filtrate in vacuo leaves dibutyl N-benzylideneaminomethylphosphonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962224 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-14da14eb265e4d97891721e41eddcede |
| Source note | uspto-grants-1976_06 |