HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzaldehyde → HCID 54329991, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzaldehyde | HCID 240 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 195283 | HCID 195283 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 54329991 | HCID 54329991 | — |
Reaction Steps
A solution of diphenyl aminomethylphosphonate (102.8 g) and benzaldehyde (41.6 g) in benzene (1000 ml) is heated at reflux in a Dean-Stark apparatus until water separation ceases. The resulting solution is evaporated under reduced pressure to yield diphenyl N-benzylideneaminomethylphosphonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962224 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-faefaa47c1854b7f9d653d462dfc1b5f |
| Source note | uspto-grants-1976_06 |