HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Ethyl-2-nitroaniline → 4-Ethylbenzene-1,2-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Ethyl-2-nitroaniline | HCID 251674 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Ethylbenzene-1,2-diamine | HCID 12373213 | — |
Reaction Steps
The crude 2-nitro-4-ethylaniline was hydrogenated in 100 ml. of ethanol over 500 mg. of 5 percent palladium on charcoal, until gas uptake ceased. The reaction mixture was filtered and evaporated, yielding 4-ethyl-o-phenylenediamine as a dark oil which solidified overnight. The identity of the product was confirmed by IR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03962440 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-6fdf5b16bcab4a59ae413857dc90c073 |
| Source note | uspto-grants-1976_06 |