HCID 12223719, compound → HCID 12223724, compound

HRID 1658069Notes

Reaction equation

[OH:1][CH:2]([CH2:27][OH:28])[CH2:3][N:4]1[C:24](=[O:25])[C:8]2[CH:9]=[CH:10][CH:11]=[C:12]3[S:13][C:14]4[CH:15]=[CH:16][C:17]([C:20]([F:23])([F:22])[F:21])=[CH:18][C:19]=4[N:6]([C:7]=23)[C:5]1=[O:26].C(Cl)(Cl)Cl.C[OH:34]>>[OH:1][CH:2]([CH2:27][OH:28])[CH2:3][N:4]1[C:24](=[O:25])[C:8]2[CH:9]=[CH:10][CH:11]=[C:12]3[S:13](=[O:34])[C:14]4[CH:15]=[CH:16][C:17]([C:20]([F:21])([F:22])[F:23])=[CH:18][C:19]=4[N:6]([C:7]=23)[C:5]1=[O:26]

Participants

Reactant 2

HCID 12223719HCID 12223719, compound

HCID 21584188Chloroform methanol

Product 1

HCID 12223724HCID 12223724, compound

Procedure

Reaction of 2-(2,3-dihydroxypropyl)-10-trifluoromethyl-1H-pyrimido[5,4,3-kl] phenothiazine-1,3(2H)-dione and m-chloroperbenozic acid according to the procedure of Example 6 gave the title compound, m.p. 224°-225° (chloroform-methanol).

Sources & evidence

ORD record: ord-41da5d2ce2b049afac2fe0bb9b0d4d65
Source dataset: uspto-grants-1976_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03962438

Reaction notes

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